Article Sidebar
Published:
Sep 18, 2015Keywords:
Article Details
Copyright for articles published in this journal is retained by the journal.
SAJChem applies the Creative Commons Attribution (CC BY) license to manuscripts we publish. This license was developed to facilitate open access – namely, free immediate access to, and unrestricted reuse of, original works of all types. Under this license, authors agree to make articles legally available for reuse, without permission or fees, for virtually any purpose. Anyone may copy, distribute or reuse these articles, as long as the author and original source are properly cited.
Main Article Content
Synthesis and Structural Studies of Nanocrystalline Cd0.3Zn0.7Fe2O4
Abstract
The synthesis of Cd0.3Zn0.7Fe2O4 nanoparticles has been achieved by a simple thermal decomposition method from the inorganic precursor, Cdd0.3Zn0.7Fe2(cin)3(N2H4)2, which was obtained by a novel precipitation method from the corresponding metal salts, cinnamic acid and hydrazine hydrate. The precursor was characterized by hydrazine and metal analyses, infrared spectral analysis and thermogravimetric analysis. Under appropriate annealing conditions, Cd0.3Zn0.7Fe2(cin)3(N2H4)2 yielded Cd0.3Zn0.7Fe2O4 nanoparticles, which were characterized for their size and structure using X-Ray Diffraction (XRD), High Resolution Transmission ElectronMicroscopic(HRTEM),SelectedArea ElectronDiffraction(SAED)andScanning ElectronMicroscopic(SEM)techniques.
KEYWORDS: Cd0.3Zn0.7Fe2O4 nanoparticles, XRD, HRTEM, SAED, SEM.
